Abstract # I-41

Purification and Characterization of Excreted and Acid Extractable Anti-Listerial Enterocin B108 Produced by Enterococcus Faecium 108.. H.L. Dallas, V. Sathyamoorthy, and A.D. Hitchins, Food and Drug Administration, Washington, DC 20204

Enterococcus faecium 108 was isolated from food by the FDA³s Listeria selective enrichment procedure. E. faecium 108 produces an extracellular anti-listerial compound, enterocin B108. The anti-listerial compound is a protein being inactivated by treatment with proteinase K, trypsin and chymotrypsin. It is active against all Listeria species, heat stable (90°C for 30 min) and is very stable during storage at -70° to 5°C. Enterocin B108 is rapidly bacteriocidal without cytolysis. However, eventually membrane damage becomes evident in electron micrographs. The approximate molecular weight (M.W.) was 10,000 by SDS-PAGE. Enterocin B108 was purified to electrophoretic homogeneity by gel-filtration, ion exchange and reverse phase chromatography using the Fast Protein Liquid Chromatography system, although the yield was insufficient to determine the sequence. Poor yield was due to interference by a pigment-like compound in the growth medium. Anti-listerial activity that is free of pigment was obtained in high yield by adjustment of washed cells to pH 2 with phosphoric acid (5% v/v). A subsequent one-step purification by gel-filtration in 5M urea produced a homogeneous protein of M.W. 10,000.