Four rapid solid phase extraction (SPE) methods were evaluated for the determination of organochlorine and organophosphorus pesticide residues in raw and homogenized milk. Pesticide residues were partitioned onto C18 SPE columns, and subsequently eluted using small volumes of organic solvents. The methods evaluated required minimal volumes of solvent (<60 mL per sample) and resulted in the production of small volumes of hazardous waste (60-120 mL). Gas chromatography with electron capture and flame photometric detection were used to quantify fortified (0.01 ppm-0.2 ppm) organochlorine and organophosphorus pesticide residues, respectively. Recovery data is presented for 24 organochlorine and 30 organophosphorus pesticide residues. Some of the parameters studied were disruption of the milk fat globule, volume and type of elution solvents, limits of detection, amount of interference from matrix coextractants. Some of the methods are suitable for homogenized milk only while others are suitable for both homogenized and raw milk.